We have made available some pulse programs suitable for carrying out some of the new NMR experiments described in our publications. The programs were written for Bruker Avance spectrometers. The pulse programs can be obtained by clicking on the links below.

WARNING

These pulse programs are intended only as guides. We do not guarantee in any way that they will necessarily work. Note especially that misuse of the pulse programs can result in serious damage to your equipment. All the parameters must be carefully adjusted to correspond to your particular spectrometer before use. By copying any of the pulse programs in our library you accept that we are in no way responsable for any loss or damage consequent to their use.

INADEQUATE Experiments in solids

• Pulse program for INADEQUATE experiments in solids (updated 2002), and the corresponding paper.
• Pulse program for Refocused INADEQUATE experiments in solids (updated 2002), and the corresponding paper.

Heteronuclear Correlation Experiments in solids

• Pulse program for HMQC experiments in solids (updated 2002), and the corresponding paper.
• Pulse program for HSQC experiments in solids (updated 2002), and the corresponding paper.
• Pulse program for refocused INEPT experiments in solids (updated 2006).
• Pulse program for Dipolar HETCOR experiments in solids with refocusing of the heteronuclear J couplings (updated 2002),
  and the corresponding paper.
• Pulse program for J-Wise experiments in solids (updated 2004), and the corresponding paper.
• Pulse program for J-Wise constant time experiments in solids (updated 2004), and the corresponding paper.
• Pulse program for Measurement of ¹⁵N Longitudinal Relaxation in solids (updated 2004).

Experiments for measuring scalar couplings in solids

• Pulse program for recording rotor synchronised homonuclear J resolved spectra (updated 2002), and the corresponding paper.
• Pulse program for 2D spin-echo experiments for measurement of homonuclear J couplings (updated 2004).
• Pulse program for pseudo-2D homonuclear experiment for selective observation of a pure J modulation in fully enriched multispin system (updated 2006).
• Pulse program for measuring J modulation between a selected pair of J-coupled spins in partially enriched multi-spin systems (updated 2006).

Spectral Editing Experiments in solids

• Pulse program for APT type Spectral Editing in solids (updated 2002), and the corresponding paper.
• Pulse program for "1Q" Multiple-Quantum Filtered Spectral Editing experiments in solids (updated 2002), and the corresponding paper.
• Pulse program for "2Q" Multiple-Quantum Filtered Spectral Editing experiments in solids (updated 2002), and the corresponding paper.
• Pulse program for "3Q" Multiple-Quantum Filtered Spectral Editing experiments in solids (updated 2002), and the corresponding paper.

IPAP Experiments in solids

• Pulse programs for In-Phase and Anti-Phase 1D IPAP spin state selective detection in solids.
• Pulse programs (in-anti, in-in, anti-in, and anti-anti) for Double-IPAP spin state selective 1D detection in solids.
• Pulse programs (i1, i2, a1, and a2) for 2D COCA-IPAP-PDSD experiment in solids.

Direct Spectral Optimization for improved decoupling schemes in solids

• Package for direct spectral optimization (eDROOPY/eDUMBO decoupling), (updated 2004), and the corresponding paper.

Proton high-resolution NMR Spectroscopy in Solids

• Pulse program for 2D proton-proton indirectly detected CRAMPS experiments in solids (recommended, for use with DUMBO decoupling) (updated 2003) and cpd file, and the corresponding paper.
• Pulse program for 1D experiment to calibrate the direction of the effective decoupling field (updated 2003), and the corresponding paper.
• Pulse program for 2D proton-proton indirectly detected CRAMPS experiments in solids (previous version, with FSLG decoupling) (updated 2002), and the corresponding paper.
• Pulse program for 2D proton-proton Constant Time CRAMPS experiments in solids (updated 2002), and the corresponding paper.
• Pulse program for 3D proton-proton-proton spin diffusion experiments in solids (updated 2002), and the corresponding paper.
• Pulse program for 3D proton-proton-carbon spin diffusion experiments in solids (updated 2002), and the corresponding paper.
• Pulse program for 1D CRAMPS experiment in solids, with windowed acquisition (updated 2003), and the corresponding paper.
• Pulse program for 2D CRAMPS experiment in solids (updated 2004).
• Pulse program for 2D Double Quantum (with POST-C7) CRAMPS experiment in solids (updated 2004).
• Pulse program (NEW) for 2D Triple Quantum (with POST-C7, homonuclear decoupling during t1) experiment in solids (updated 2007).

Homonuclear Dipolar Decoupling in Solids

• C program for creation of phase files for DUMBO-1 homonuclear decoupling (to be used with an input seed file) (updated 2003), and the corresponding paper.
• Input seed file for DUMBO-1 or eDUMBO-1₂₂ decoupling (to be used together with C program for creating phase files) (updated 2006).
• Exemples of phase files:
  - Phase file (256 cycles, 64 steps per cycle) of DUMBO-1 for homonuclear decoupling experiments in solids (updated 2003)
  - Phase file (2 cycles, 64 steps per cycle) of DUMBO-1 for homonuclear decoupling experiments in solids (updated 2003)
  
• CPD file (decshape) for DUMBO/eDUMBO homonuclear decoupling (windowless).
  

Correlation of fast and slow CSA spinning sideband patterns in Solids

• Pulse program for 2D ROSES experiment in solids (updated 2002), and the corresponding paper.